Fact Snapshot
- Paper: Ultrasonic–microwave synergistic liquid–liquid microextraction based on solidified floating organic droplets for extraction of histamine in beer and fish and exploration of the extraction process
- Equipment: XH-300A+ and XH-300 series
- Source: LWT - Food Science and Technology, 2024
- Research direction: food-safety testing, histamine detection, and sample pretreatment
- Key results: Inter-day precision 0.81%, Precision 0.86%, and Recovery 94.28%
Research Abstract
Ultrasonic–microwave synergistic liquid–liquid microextraction based on solidified floating organic droplets for extraction of histamine in beer and fish and exploration of the extraction process was published in LWT - Food Science and Technology (2024) and is indexed as a Xianghu Q1 application case for XH-300A+ and XH-300 series. The structured source links this paper to food-safety testing, histamine detection, and sample pretreatment. Key reported results include Inter-day precision 0.81%, Precision 0.86%, and Recovery 94.28%. The DOI recorded for this paper is 10.1016/j.lwt.2024.115932.
Research Background and Problem
Key Result
| Metric | Result |
|---|---|
| Inter-day precision | 0.81% |
| Precision | 0.86% |
| Recovery | 94.28% |
Evidence Details
the intra-day precision is 0.86%–1.22% and 0.98%–2.11%, and the inter-day precision is 0.81%–1.75% and 1.45%–2.32%
The linear range of this method in combination with visible spectrophotometry for the determination of His in beer and fish is 0.3–15 mg L−1 and 1–300 mg kg−1, limit of detection is 0.1 mg L−1 and 0.3 mg kg−1
The UMS extraction was performed using an XH-300A+ ultrasonic microwave combination synthesis/extraction instrument (Beijing XiangHu Science and Technology Development Co., Ltd., Beijing, China).
Under this condition, the recovery was 94.28%.
Mechanism / Method Highlights
- Source evidence: the intra-day precision is 0.86%–1.22% and 0.98%–2.11%, and the inter-day precision is 0.81%–1.75% and 1.45%–2.32%
- Abstract evidence: The linear range of this method in combination with visible spectrophotometry for the determination of His in beer and fish is 0.3–15 mg L−1 and 1–300 mg kg−1, limit of detection is 0.1 mg L−1 and 0.3 mg kg−1
- Equipment evidence: The UMS extraction was performed using an XH-300A+ ultrasonic microwave combination synthesis/extraction instrument (Beijing XiangHu Science and Technology Development Co., Ltd., Beijing, China)
- Reported outcome: Inter-day precision 0.81%, Precision 0.86%, and Recovery 94.28%.
Application Value
- Positions XH-300A+ and XH-300 series in a peer-reviewed Q1 research application.
- Highlights quantitative evidence: Inter-day precision 0.81%, Precision 0.86%, and Recovery 94.28%.
- Records source affiliations: Northeast Agricultural University and College of Food Science, Northeast Agricultural University, Harbin 150030, China.
Related Equipment
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Ultrasonic–microwave synergistic liquid–liquid microextraction based on solidified floating organic droplets for extraction of histamine in beer and fish and exploration of the extraction process
LWT - Food Science and Technology, 2024
DOI: 10.1016/j.lwt.2024.115932
