Fact Snapshot
- Paper: 2D Co3O4 modified by IrO2 nanozyme for convenient detection of aqueous Fe2+ and intercellular H2O2
- Equipment: XH-MC-1
- Source: Microchimica Acta, 2023
- Research direction: nanozyme sensing, visual paper-strip detection, microwave material synthesis, and biomedical analysis
- Core conditions: Temperature 140 ℃
- Key results: Recovery 101.2%, Recovery 102.5%, and Recovery 103.7%
Research Abstract
2D Co3O4 modified by IrO2 nanozyme for convenient detection of aqueous Fe2+ and intercellular H2O2 was published in Microchimica Acta (2023) and is indexed as a Xianghu Q1 application case for XH-MC-1. The source record connects it with nanozyme sensing, visual paper-strip detection, microwave material synthesis, and biomedical analysis. Core operating conditions include Temperature 140 ℃. Key reported results include Recovery 101.2%, Recovery 102.5%, and Recovery 103.7%.
Research Background and Problem
Equipment Use and Experimental Conditions
| Item | Parameter |
|---|---|
| Temperature | 140 ℃ |
Key Result
| Metric | Result |
|---|---|
| Recovery | 101.2% |
| Recovery | 102.5% |
| Recovery | 103.7% |
Evidence Details
Release-kinetics evidence: source values include R2 = 0.9927, R2 = 0.9982.
Additional source evidence: source values include 8 mol/L, 7 mol/L, 101.2%, 102.5%, 95.8%, 103.7%.
The recoveries were 101.2 ~ 102.5% and 95.8 ~ 103.7% with detection limits of 1.25 × 10−8 mol/L and 1.02 × 10−7 mol/L, respectively.
Microwave synthesis was conducted in a XH-MC-1 microwave reactor at 700 W (Beijing Xianghu Science and Technology Development Co., LTD).
Microwave-method evidence: source values include 700 W, 140 °C. Entities: XH-MC-1.
Under the optimized conditions (pH 4.0, 0.08 mM TMB, and incubated for 4.0 min at 25 °C), it could accelerate the redox of TMB and H2O2 with Km/Vmax of 0.091 mM/1.615 × 10−7 M·s−1 and 0.065 mM/1.131 × 10−7 M·s−1.
Mechanism / Method Highlights
- Method context: Temperature 140 ℃.
- Release-kinetics evidence: source values include R2 = 0.9927, R2 = 0.9982
- Additional source evidence: source values include 8 mol/L, 7 mol/L, 101.2%, 102.5%, 95.8%, 103.7%
- Source evidence: The recoveries were 101.2 ~ 102.5% and 95.8 ~ 103.7% with detection limits of 1.25 × 10−8 mol/L and 1.02 × 10−7 mol/L, respectively
- Reported outcome: Recovery 101.2%, Recovery 102.5%, and Recovery 103.7%.
Application Value
- XH-MC-1 IrO2@2D Co3O4
- Fe2+ 1.25 × 10−8 mol/L, H2O2 1.02 × 10−7 mol/L, respectively 101.2%~102.5% 95.8%~103.7%
Related Equipment
FAQ
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2D Co3O4 modified by IrO2 nanozyme for convenient detection of aqueous Fe2+ and intercellular H2O2
Microchimica Acta, 2023
DOI: 10.1007/s00604-022-05582-1
