Fact Snapshot
- Paper: Microwave-Assisted Rapid Synthesis of Bismuth Molybdate with Enhanced Oxidative Desulfurization Activity
- Equipment: XH-300PE
- Source: Fuel, 2022
- Research direction: microwave hydrothermal synthesis
- Core conditions: Temperature 60 ℃ / 160 ℃ and Time 12 h / 30 min
- Key results: Removal 99.68%, Removal 99.71%, and Removal 77.95%
Research Abstract
Microwave-Assisted Rapid Synthesis of Bismuth Molybdate with Enhanced Oxidative Desulfurization Activity was published in Fuel (2022) and is indexed as a Xianghu Q1 application case for XH-300PE. The structured source links this paper to microwave hydrothermal synthesis. Core operating conditions include Temperature 60 ℃ / 160 ℃ and Time 12 h / 30 min. Key reported results include Removal 99.68%, Removal 99.71%, and Removal 77.95%. The DOI recorded for this paper is 10.1016/j.fuel.2022.125900.
Research Background and Problem
Equipment Use and Experimental Conditions
| Item | Parameter |
|---|---|
| Temperature | 60 ℃ / 160 ℃ |
| Time | 12 h / 30 min |
Key Result
| Metric | Result |
|---|---|
| Removal | 99.68% |
| Removal | 99.71% |
| Removal | 77.95% |
| Removal | 98.07% |
| Conversion | 33.98% |
Evidence Details
Equipment-detail evidence: source values include 33.98%, 0.025 g, 1:2, 15 min, 99.71%, 50 °C, 60 °C, 70 °C, 98.14%. Entities: BMO-1.
the obtained precursor suspension was transferred into a 100 mL Teflon reactor which was placed into an XH-300PE high-pressure microwave hydrothermal synthesizer ... and heated at 160 ℃ for 30 min.
The sample prepared at pH 1, BMO-1, exhibited superior activity for oxidizing sulfur compounds in fuel oil at 60 ℃ with a molar hydrogen peroxide to sulfur ratio of four, achieving removal rates of dibenzothiophene, 4,6-dimethyldibenzothiophene, and benzothiophene of 99.71%, 99.68%, and 77.95%, respectively.
Microwave-method evidence: source values include 40 °C, 80 °C, 12 h. Entities: XH-300PE, BMO-X.
Additional source evidence: source values include 99.5%, 15 min, 59.14%. Entities: BMO-1, BMO-X, BMO-11.
the removal rate of DBT can still reach 98.07% after 7 cycles, indicating good desulfurization performance stability of the BMO-1 catalyst.
Additional source evidence: source values include 0.188726 mL, 20.1353 nm. Entities: BMO-1.
Additional source evidence: source values include 5 mL, 30 min. Entities: GC-FID.
Additional source evidence: source values include 10 mL, 60 mL.
Mechanism / Method Highlights
- Method context: Temperature 60 ℃ / 160 ℃ and Time 12 h / 30 min.
- Equipment-detail evidence: source values include 33.98%, 0.025 g, 1:2, 15 min, 99.71%, 50 °C, 60 °C, 70 °C, 98.14%. Entities: BMO-1
- Equipment evidence: the obtained precursor suspension was transferred into a 100 mL Teflon reactor which was placed into an XH-300PE high-pressure microwave hydrothermal synthesizer ... and heated at 160 ℃ for 30 min
- Abstract evidence: The sample prepared at pH 1, BMO-1, exhibited superior activity for oxidizing sulfur compounds in fuel oil at 60 ℃ with a molar hydrogen peroxide to sulfur ratio of four, achieving removal rates of dibenzothiophene, 4,6-dimethyldibenzothiophene, and benzothiophene of 99.71%, 99.68%, and 77.95%, respectively
- Reported outcome: Removal 99.68%, Removal 99.71%, Removal 77.95%, and Removal 98.07%.
Application Value
- Positions XH-300PE in a peer-reviewed Q1 research application.
- Highlights quantitative evidence: Removal 99.68%, Removal 99.71%, and Removal 77.95%.
- Records source affiliations: Guangdong Institute of Petrochemical Technology and College of Materials and Chemistry & Chemical Engineering, Chengdu University of Technology, Chengdu 610059, China.
Related Equipment
FAQ
Which Xianghu instrument is covered by this page?
What is the main application direction?
Which publication does this case come from?
Microwave-Assisted Rapid Synthesis of Bismuth Molybdate with Enhanced Oxidative Desulfurization Activity
Fuel, 2022
DOI: 10.1016/j.fuel.2022.125900