Q1 Research Application · Frontier Focus

Designed 3D N-doped magnetic porous carbon spheres for sensitive monitoring of biogenic amine by simultaneous microwave-assisted derivatization and magnetic-solid phase extraction

This Journal of Chromatography A paper (2022) is indexed as a SoarNova / Xianghu equipment application case for XH-100A; key results include Recovery -108.8%.

View DOI Back to Library Chinese Solution
Paper ID 466
Application Focus Food-safety testing, Sample pretreatment
Key Result Recovery -108.8%
Core Condition Temperature 800 ℃
Paper ID
466
Journal
Journal of Chromatography A
Impact Factor
4.759
CAS Zone
Zone 1
Year
2022
DOI
10.1016/j.chroma.2022.462882
Equipment Model
XH-100A
Affiliations
Liaoning University; College of Chemistry, Liaoning University, Shenyang 110036, China; Department of Mechanical and Power Engineering, Yingkou Institute of Technology, Yingkou 115014, China; Ecology and Environmental Monitoring Center of Jilin Province, Changchun 130011, China
Research Directions
Food-safety testing Sample pretreatment

Fact Snapshot

  • Paper: Designed 3D N-doped magnetic porous carbon spheres for sensitive monitoring of biogenic amine by simultaneous microwave-assisted derivatization and magnetic-solid phase extraction
  • Equipment: XH-100A
  • Source: Journal of Chromatography A, 2022
  • Research direction: Food-safety testing and Sample pretreatment
  • Core conditions: Temperature 800 ℃, Microwave power 200 W, and Time 3 h
  • Key results: Recovery -108.8%

Research Abstract

Designed 3D N-doped magnetic porous carbon spheres for sensitive monitoring of biogenic amine by simultaneous microwave-assisted derivatization and magnetic-solid phase extraction was published in Journal of Chromatography A (2022) and is indexed as a SoarNova / Xianghu Q1 application case for XH-100A. The source record connects it with Food-safety testing and Sample pretreatment. Core operating conditions include Temperature 800 ℃, Microwave power 200 W, and Time 3 h. Key reported results include Recovery -108.8%.

Research Background and Problem

The paper is positioned around food-safety testing and sample pretreatment. The equipment record identifies XH-100A as the Xianghu instrument context for this application case. The source affiliation record includes Liaoning University and College of Chemistry, Liaoning University, Shenyang 110036, China.

Equipment Use and Experimental Conditions

ItemParameter
Temperature800 ℃
Microwave power200 W
Time3 h

Key Result

Recovery -108.8%
MetricResult
Recovery-108.8%

Evidence Details

Release-kinetics evidence

Release-kinetics evidence: source values include R2 = 0.9943, R2 = 0.9995, R2 = 0.059. Entities: LC-HRMS.

Microwave-method evidence

Microwave-method evidence: source values include 40 mL, 20 mg, 200 W, 135 s, 4 mL, 2 mL, 4 min. Entities: XH-100B, MAD-MSPE, N-MPCSs, DNS-Cl.

Source evidence

The RSDs of the samples were in the range of 1.5–5.9%, and the recovery was in the range of 92.3–108.8%.

Microwave-method evidence

Microwave-method evidence: source values include 15 min, 10 min.

Additional source evidence

Additional source evidence: source values include 800 °C, 3 h. Entities: N-MPCSs.

Structured key result

Recovery: -108.8%

Mechanism / Method Highlights

  • Method context: Temperature 800 ℃, Microwave power 200 W, and Time 3 h.
  • Release-kinetics evidence: source values include R2 = 0.9943, R2 = 0.9995, R2 = 0.059. Entities: LC-HRMS
  • Microwave-method evidence: source values include 40 mL, 20 mg, 200 W, 135 s, 4 mL, 2 mL, 4 min. Entities: XH-100B, MAD-MSPE, N-MPCSs, DNS-Cl
  • Source evidence: The RSDs of the samples were in the range of 1.5–5.9%, and the recovery was in the range of 92.3–108.8%
  • Reported outcome: Recovery -108.8%.

Application Value

  • Provides a peer-reviewed SoarNova / Xianghu Q1 application case for XH-100A.
  • Supports English discovery around Food-safety testing and Sample pretreatment.
  • Preserves quantitative result evidence: Recovery -108.8%.
  • Maintains source-level evidence details: Release-kinetics evidence: source values include R2 = 0.9943, R2 = 0.9995, R2 = 0.059. Entities: LC-HRMS, Microwave-method evidence: source values include 40 mL, 20 mg, 200 W, 135 s, 4 mL, 2 mL, 4 min. Entities: XH-100B, MAD-MSPE, N-MPCSs, DNS-Cl, Source evidence: The RSDs of the samples were in the range of 1.5–5.9%, and the recovery was in the range of 92.3–108.8%, and Microwave-method evidence: source values include 15 min, 10 min.

Related Equipment

XH-100A+ Microwave Catalytic Synthesis/Extraction System
XH-100A+ Microwave Catalytic Synthesis/Extraction System

FAQ

Which Xianghu instrument is covered by this page?
The structured source records XH-100A for this paper.
What is the main application direction?
The source tags this paper under food-safety testing and sample pretreatment.
Which publication does this case come from?
It comes from Journal of Chromatography A (2022), DOI 10.1016/j.chroma.2022.462882.
Citation
Designed 3D N-doped magnetic porous carbon spheres for sensitive monitoring of biogenic amine by simultaneous microwave-assisted derivatization and magnetic-solid phase extraction
Journal of Chromatography A, 2022
DOI: 10.1016/j.chroma.2022.462882