Fact Snapshot
- Paper: Facile microwave-assisted synthesis of Ti3C2 MXene quantum dots for ratiometric fluorescence detection of hypochlorite
- Equipment: XH-100A
- Source: MICROCHIMICA ACTA, 2020
- Research direction: MXene
- Core conditions: Temperature 40°C / 60°C / 90°C, Microwave power 800 W, and Time 12 h / 3 min / 5 min
- Key results: Diameter 2 nm
Research Abstract
Facile microwave-assisted synthesis of Ti3C2 MXene quantum dots for ratiometric fluorescence detection of hypochlorite was published in MICROCHIMICA ACTA (2020) and is indexed as a Xianghu Q1 application case for XH-100A. The source record connects it with MXene. Core operating conditions include Temperature 40°C / 60°C / 90°C, Microwave power 800 W, and Time 12 h / 3 min / 5 min. Key reported results include Diameter 2 nm.
Research Background and Problem
Equipment Use and Experimental Conditions
| Item | Parameter |
|---|---|
| Temperature | 40°C / 60°C / 90°C |
| Microwave power | 800 W |
| Time | 12 h / 3 min / 5 min |
Key Result
| Metric | Result |
|---|---|
| Diameter | 2 nm |
Evidence Details
Release-kinetics evidence: source values include R² = 0.991, R2 = 0.991.
The linear detection range of curcumin was 0.05–10 μM, and the detection limit was 20 nM. The linear detection ranges of ClO⁻ are 25–150 μM and 150–275 μM, and the detection limit is 5 μM.
The round bottom flask was placed in a microwave reactor under microwave-assisted irradiation (800 W, 90 °C) for 5 min.
Additional source evidence: source values include 300 nm, 430 nm, 420 nm, 510 nm.
Additional source evidence: source values include 1 g, 16 mL, 40°C, 24 h.
Additional source evidence: source values include 0.05–10 μM, 1 mg/mL, 2 mL.
Additional source evidence: source values include 1 mg/mL, 25–325 μM, 2 mL.
Additional source evidence: source values include 100 mg, 50 mL, 100 mL.
Temperature: 40°C / 60°C / 90°C
Time: 12 h / 3 min / 5 min
The XH-100A computer microwave catalytic synthesis extraction instrument was used to synthesize Ti₃C₂ MQDs (Beijing Xianghu Technology Co., Ltd., China, http://www.xianghukeji.com/).
Microwave-method evidence: source values include 6–12 h, 5 min.
Additional source evidence: source values include 430 nm, 540 nm.
Additional source evidence: source values include 330 nm, 20 nm.
Mechanism / Method Highlights
- Method context: Temperature 40°C / 60°C / 90°C, Microwave power 800 W, and Time 12 h / 3 min / 5 min.
- Release-kinetics evidence: source values include R² = 0.991, R2 = 0.991
- Source evidence: The linear detection range of curcumin was 0.05–10 μM, and the detection limit was 20 nM. The linear detection ranges of ClO⁻ are 25–150 μM and 150–275 μM, and the detection limit is 5 μM
- Source evidence: The round bottom flask was placed in a microwave reactor under microwave-assisted irradiation (800 W, 90 °C) for 5 min
- Reported outcome: Diameter 2 nm.
Application Value
- Provides a peer-reviewed SoarNova / Xianghu Q1 application case for XH-100A.
- Supports English discovery around MXene.
- Preserves quantitative result evidence: Diameter 2 nm.
- Maintains source-level evidence details: Release-kinetics evidence: source values include R² = 0.991, R2 = 0.991, Source evidence: The linear detection range of curcumin was 0.05–10 μM, and the detection limit was 20 nM. The linear detection ranges of ClO⁻ are 25–150 μM and 150–275 μM, and the detection limit is 5 μM, Source evidence: The round bottom flask was placed in a microwave reactor under microwave-assisted irradiation (800 W, 90 °C) for 5 min, and Additional source evidence: source values include 300 nm, 430 nm, 420 nm, 510 nm.
Related Equipment
FAQ
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Facile microwave-assisted synthesis of Ti3C2 MXene quantum dots for ratiometric fluorescence detection of hypochlorite
MICROCHIMICA ACTA, 2020
DOI: 10.1007/s00604-020-04668-y