Q1 Research Application · Frontier Focus

Microwave-Assisted Synthesis of NiCo2O4 Double-Shelled Hollow Spheres for High-Performance Sodium Ion Batteries

This nano-micro letters paper (2017) is indexed as a Xianghu equipment application case for XH-800S; key result: Specific surface area 30.7 m² g-1.

View DOI Back to Library Chinese Solution
Paper ID 356
Application Focus NiCo₂O₄, microwave-assisted solvothermal synthesis, Anode material
Key Result Specific surface area 30.7 m² g-1
Core Condition Temperature 180°C
Paper ID
356
Journal
nano-micro letters
Impact Factor
7.4
CAS Zone
Zone 1
Year
2017
DOI
10.1007/s40820-017-0164-2
Equipment Model
XH-800S
Affiliations
Sichuan University; School of Chemical Engineering, Sichuan University, Chengdu 610065, People's Republic of China; School of Electronics and Information Engineering, Sichuan University, Chengdu 610065, People's Republic of China
Research Directions
NiCo₂O₄ microwave-assisted solvothermal synthesis Anode material

Fact Snapshot

  • Paper: Microwave-Assisted Synthesis of NiCo2O4 Double-Shelled Hollow Spheres for High-Performance Sodium Ion Batteries
  • Equipment: XH-800S
  • Source: nano-micro letters, 2017
  • Research direction: NiCo₂O₄, microwave-assisted solvothermal synthesis, and anode material
  • Core conditions: Temperature 180°C and Time 30 min / 20 min / 6 h
  • Key results: Specific surface area 30.7 m² g-1, Capacitance 341 mAh g-1, and Specific capacity 511 mAh g-1

Research Abstract

Microwave-Assisted Synthesis of NiCo2O4 Double-Shelled Hollow Spheres for High-Performance Sodium Ion Batteries was published in nano-micro letters (2017) and is indexed as a Xianghu Q1 application case for XH-800S. The structured source links this paper to NiCo₂O₄, microwave-assisted solvothermal synthesis, and anode material. Core operating conditions include Temperature 180°C and Time 30 min / 20 min / 6 h. Key reported results include Specific surface area 30.7 m² g-1, Capacitance 341 mAh g-1, and Specific capacity 511 mAh g-1. The DOI recorded for this paper is 10.1007/s40820-017-0164-2.

Research Background and Problem

The paper is positioned around NiCo₂O₄, microwave-assisted solvothermal synthesis, and anode material. The equipment record identifies XH-800S as the Xianghu instrument context for this application case. The source affiliation record includes Sichuan University and School of Chemical Engineering, Sichuan University, Chengdu 610065, People's Republic of China.

Equipment Use and Experimental Conditions

ItemParameter
Temperature180°C
Time30 min / 20 min / 6 h

Key Result

Specific surface area 30.7 m² g-1
Capacitance 341 mAh g-1
Specific capacity 511 mAh g-1
Coulombic efficiency 63%
MetricResult
Specific surface area30.7 m² g-1
Capacitance341 mAh g-1
Specific capacity511 mAh g-1
Coulombic efficiency63%
Retention66%
Annealed diameter1 μm

Evidence Details

Release-kinetics evidence

Release-kinetics evidence: source values include R2032, 8:1, 12 h, 1 mg, 1:1, R2 = 1.

Microwave-method evidence

Microwave-method evidence: source values include 80 mL, 16 mL, 30 min, 60 mL, 100 mL, 180°C, 20 min, 350°C, 2 h, 1°C. Entities: XH-800G.

Additional source evidence

Additional source evidence: source values include 350°C, 1°C, 300–400 nm, 20 nm, 70 nm.

Release evidence

Release evidence: source values include 180°C, 2H, 30 min, 6 h.

Additional source evidence

Additional source evidence: source values include 1 μm, 5°C, 10°C.

Stability evidence

Stability evidence: source values include 66%, 98%.

Structured key result

Coulombic efficiency: 63%

Mechanism / Method Highlights

  • Method context: Temperature 180°C and Time 30 min / 20 min / 6 h.
  • Release-kinetics evidence: source values include R2032, 8:1, 12 h, 1 mg, 1:1, R2 = 1
  • Microwave-method evidence: source values include 80 mL, 16 mL, 30 min, 60 mL, 100 mL, 180°C, 20 min, 350°C, 2 h, 1°C. Entities: XH-800G
  • Additional source evidence: source values include 350°C, 1°C, 300–400 nm, 20 nm, 70 nm
  • Reported outcome: Specific surface area 30.7 m² g-1, Capacitance 341 mAh g-1, Specific capacity 511 mAh g-1, and Coulombic efficiency 63%.

Application Value

  • Positions XH-800S in a peer-reviewed Q1 research application.
  • Highlights quantitative evidence: Specific surface area 30.7 m² g-1, Capacitance 341 mAh g-1, and Specific capacity 511 mAh g-1.
  • Records source affiliations: Sichuan University and School of Chemical Engineering, Sichuan University, Chengdu 610065, People's Republic of China.

Related Equipment

XH-800SE Microwave Hydrothermal Synthesizer
XH-800SE Microwave Hydrothermal Synthesizer

FAQ

Which Xianghu instrument is covered by this page?
The structured source records XH-800S for this paper.
What is the main application direction?
The source tags this paper under NiCo₂O₄, microwave-assisted solvothermal synthesis, and anode material.
Which publication does this case come from?
It comes from nano-micro letters (2017), DOI 10.1007/s40820-017-0164-2.
Citation
Microwave-Assisted Synthesis of NiCo2O4 Double-Shelled Hollow Spheres for High-Performance Sodium Ion Batteries
nano-micro letters, 2017
DOI: 10.1007/s40820-017-0164-2