Q1 Research Application · Frontier Focus

Microwave-assisted reflux rapid synthesis of MnO2 nanostructures and their application in supercapacitors

This Electrochimica Acta paper (2013) is indexed as a Xianghu equipment application case for XH-100A; key result: Retention 93%.

View DOI Back to Library Chinese Solution
Paper ID 142
Application Focus Supercapacitor electrode materials
Key Result Retention 93%
Core Condition Power 800 W
Paper ID
142
Journal
Electrochimica Acta
Impact Factor
5.116
CAS Zone
Zone 1
Year
2013
DOI
10.1016/j.electacta.2012.10.022
Equipment Model
XH-100A
Affiliations
Chinese Academy of Sciences
Research Directions
Supercapacitor electrode materials

Fact Snapshot

  • Paper: Microwave-assisted reflux rapid synthesis of MnO2 nanostructures and their application in supercapacitors
  • Equipment: XH-100A
  • Source: Electrochimica Acta, 2013
  • Research direction: supercapacitor electrode materials
  • Core conditions: Power 800 W and Time 5 min / 10 min / 30 min
  • Key results: Retention 93%, Specific surface area 76 m2 g^-1, and Specific surface area 55 m2 g^-1

Research Abstract

Microwave-assisted reflux rapid synthesis of MnO2 nanostructures and their application in supercapacitors was published in Electrochimica Acta (2013) and is indexed as a Xianghu Q1 application case for XH-100A. The structured source links this paper to supercapacitor electrode materials. Core operating conditions include Power 800 W and Time 5 min / 10 min / 30 min. Key reported results include Retention 93%, Specific surface area 76 m2 g^-1, and Specific surface area 55 m2 g^-1. The DOI recorded for this paper is 10.1016/j.electacta.2012.10.022.

Research Background and Problem

The paper is positioned around supercapacitor electrode materials. The equipment record identifies XH-100A as the Xianghu instrument context for this application case. The source affiliation record includes Chinese Academy of Sciences.

Equipment Use and Experimental Conditions

ItemParameter
Power800 W
Time5 min / 10 min / 30 min

Key Result

Retention 93%
Specific surface area 76 m2 g^-1
Specific surface area 55 m2 g^-1
Coulombic efficiency 100%
MetricResult
Retention93%
Specific surface area76 m2 g^-1
Specific surface area55 m2 g^-1
Coulombic efficiency100%

Evidence Details

Equipment-detail evidence

Equipment-detail evidence: magnetic stirring.

Source evidence

The microwave power was set to 100% of 800 W ... to maintain the input temperature value of 98 ± 2 °C with a hold time of 5-30 min.

Condition evidence

Time: 5 min / 10 min / 30 min

Equipment evidence

The mixture was transferred into a 250 cm3 round-bottomed flask and placed in XH-100B (Beijing, Xianghu Co.) microwave oven fitted with a reflux condenser...

Structured key result

Retention: 93%

Mechanism / Method Highlights

  • Method context: Power 800 W and Time 5 min / 10 min / 30 min.
  • Equipment-detail evidence: magnetic stirring
  • Source evidence: The microwave power was set to 100% of 800 W ... to maintain the input temperature value of 98 ± 2 °C with a hold time of 5-30 min
  • Condition evidence: Time: 5 min / 10 min / 30 min
  • Reported outcome: Retention 93%, Specific surface area 76 m2 g^-1, Specific surface area 55 m2 g^-1, and Coulombic efficiency 100%.

Application Value

  • Positions XH-100A in a peer-reviewed Q1 research application.
  • Highlights quantitative evidence: Retention 93%, Specific surface area 76 m2 g^-1, and Specific surface area 55 m2 g^-1.
  • Records source affiliations: Chinese Academy of Sciences.

Related Equipment

XH-100A+ Microwave Catalytic Synthesis/Extraction System
XH-100A+ Microwave Catalytic Synthesis/Extraction System

FAQ

Which Xianghu instrument is covered by this page?
The structured source records XH-100A for this paper.
What is the main application direction?
The source tags this paper under supercapacitor electrode materials.
Which publication does this case come from?
It comes from Electrochimica Acta (2013), DOI 10.1016/j.electacta.2012.10.022.
Citation
Microwave-assisted reflux rapid synthesis of MnO2 nanostructures and their application in supercapacitors
Electrochimica Acta, 2013
DOI: 10.1016/j.electacta.2012.10.022