Q1 Research Application · Frontier Focus

Preparation and structural characterization of poly-mannose synthesized by phosphoric acid catalyzation under microwave irradiation

This Carbohydrate Polymers paper (2015) is indexed as a Xianghu equipment application case for XH-200A / XH-200C; key result: Yield 91.46%.

View DOI Back to Library Chinese Solution
Paper ID 10
Application Focus Research application
Key Result Yield 91.46%
Core Condition Temperature 115 °C
Paper ID
10
Journal
Carbohydrate Polymers
Impact Factor
10.723
CAS Zone
Zone 1
Year
2015
DOI
10.1016/j.carbpol.2014.12.046
Equipment Model
XH-200A / XH-200C
Affiliations
Jiangnan University; Key Laboratory of Industrial Biotechnology, Ministry of Education, Jiangnan University, Wuxi 214122, Jiangsu, PR China; State Key Laboratory of Food Science and Technology, School of Food Science and Technology, Jiangnan University, Wuxi 214122, Jiangsu, PR China
Research Directions
Research application

Fact Snapshot

  • Paper: Preparation and structural characterization of poly-mannose synthesized by phosphoric acid catalyzation under microwave irradiation
  • Equipment: XH-200A / XH-200C
  • Source: Carbohydrate Polymers, 2015
  • Research direction: Research application
  • Core conditions: Temperature 115 °C, Microwave power 900 W, and Time 5 min
  • Key results: Yield 91.46%

Research Abstract

Preparation and structural characterization of poly-mannose synthesized by phosphoric acid catalyzation under microwave irradiation was published in Carbohydrate Polymers (2015) and is indexed as a Xianghu Q1 application case for XH-200A / XH-200C. The source record connects it with Research application. Core operating conditions include Temperature 115 °C, Microwave power 900 W, and Time 5 min. Key reported results include Yield 91.46%.

Research Background and Problem

The application context is Research application. The equipment metadata identifies XH-200A / XH-200C, while the publication metadata records Carbohydrate Polymers (2015). The affiliation record includes Jiangnan University and Key Laboratory of Industrial Biotechnology, Ministry of Education, Jiangnan University, Wuxi 214122, Jiangsu, PR China. The recorded DOI is 10.1016/j.carbpol.2014.12.046.

Equipment Use and Experimental Conditions

ItemParameter
Temperature115 °C
Microwave power900 W
Time5 min

Key Result

Yield 91.46%
MetricResult
Yield91.46%

Evidence Details

Abstract evidence

The optimum reaction conditions were microwave output power of 900 W, temperature 115 °C, proton concentration 2.5 mol/L, and microwave irradiation time 5 min. The actual maximum yield was 91.46%.

Equipment and method evidence

Then the mixture was taken to the cavity of the XH-200A microwave reactor (Beijing Xianghu Science and Technology Development Co., Ltd., Beijing, China) and subjected to microwave irradiation (900 W) at 115 °C for 5 min with constant stirring.

Microwave-method evidence

Microwave-method evidence: source values include 50 g, 6 mL, 2.5 mol/L. Entities: d-mannose.

Mechanism / Method Highlights

  • Method context: Temperature 115 °C, Microwave power 900 W, and Time 5 min.
  • Abstract evidence: The optimum reaction conditions were microwave output power of 900 W, temperature 115 °C, proton concentration 2.5 mol/L, and microwave irradiation time 5 min. The actual maximum yield was 91.46%
  • Equipment and method evidence: Then the mixture was taken to the cavity of the XH-200A microwave reactor (Beijing Xianghu Science and Technology Development Co., Ltd., Beijing, China) and subjected to microwave irradiation (900 W) at 115 °C for 5 min with constant stirring
  • Microwave-method evidence: source values include 50 g, 6 mL, 2.5 mol/L. Entities: d-mannose
  • Reported outcome: Yield 91.46%.

Application Value

  • Provides a peer-reviewed SoarNova / Xianghu Q1 application case for XH-200A / XH-200C.
  • Supports English discovery around Research application.
  • Preserves quantitative result evidence: Yield 91.46%.
  • Maintains source-level evidence details: Abstract evidence: The optimum reaction conditions were microwave output power of 900 W, temperature 115 °C, proton concentration 2.5 mol/L, and microwave irradiation time 5 min. The actual maximum yield was 91.46%, Equipment and method evidence: Then the mixture was taken to the cavity of the XH-200A microwave reactor (Beijing Xianghu Science and Technology Development Co., Ltd., Beijing, China) and subjected to microwave irradiation (900 W) at 115 °C for 5 min with constant stirring, and Microwave-method evidence: source values include 50 g, 6 mL, 2.5 mol/L. Entities: d-mannose.

Related Equipment

XH-200A+ Microwave Solid-Liquid Phase Synthesis/Extraction System
XH-200A+ Microwave Solid-Liquid Phase Synthesis/Extraction System

FAQ

Which Xianghu instrument is covered by this page?
The structured source records XH-200A / XH-200C for this paper.
What research direction does this page support?
The source tags this paper under Research application.
Which publication does this case come from?
It comes from Carbohydrate Polymers (2015), DOI 10.1016/j.carbpol.2014.12.046.
Citation
Preparation and structural characterization of poly-mannose synthesized by phosphoric acid catalyzation under microwave irradiation
Carbohydrate Polymers, 2015
DOI: 10.1016/j.carbpol.2014.12.046